Zebron ZB-35HT GC Columns
High Temperature Stability for Mid-Polarity
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Zebron ZB-35HT Inferno GC Columns
High Temperature Stability for Mid-Polarity
- First non-metal, 35 % phenyl columns stable to 400 ˚C
- Longer lifetime with rugged high temperature, polyimide coated, fused silica tubing
- Robust column for high temperature analysis
- Great for high molecular weight compounds
- Eliminate carry-over with high temperature bake outs
- Low activity, provides good peak shape for acidic and basic samples
Recommended Use
Amines, Aroclors, Chemicals, Drugs, EPA Methods (508, 608, 8081, 8141, 8151), Pesticides, Pharmaceuticals, Semi-volatiles, Steroids
R&D 100 Award-Winning
Technology for High Temp Testing with advanced polymer bonding technology and specialized high temperature polyimide coating, Zebron Inferno columns offer enhanced performance where other columns fail. See how Inferno columns allow analysts to push a standard analysis up to 430 °C. Download the brochure here.
Overview
Upgrade to Zebron from any 35 % phenyl / 65 % dimethylpolysiloxane phase:
Agilent® | Restek® | SGE® | Supelco® | OV® |
|---|---|---|---|---|
DB®-35 | Rtx®-35 | BP35 | MDN-35 | OV-11 |
| DB-35ms | Rtx-35ms | BPX608 | SPB®-35 | |
| HP-35 | SPB-608 |
Lower Bleed Than Other Columns!
Great Separation of High Boiling Hydrocarbons (ASTM D6352)
Conditions for all columns:
Dimension: | 30 meter x 0.25 mm x 0.25 μm |
Detector: | FID @ 405 °C |
Injection: | Split 20:1 @ 200 °C, 1 µL |
Carrier Gas: | Helium @ 1.7 mL/min (constant flow) |
Oven Program: | 100 °C to 320 °C @ 30 °C/min for 5 min to340 °C @ 20 °C/min for 5 min to 360 °C @20 °C/min for 5 min to 380 °C @ 20 °C/minfor 5 min to 400 °C @ 20 °C/min for 5 min to 100 °C @ 30 °C/min for 8 min |
See What You’ve Been Missing
Detector: | A) FID @ 400 °CB) FID @ 320 °C |
Part No.: | 7HG-G025-11 (ZB-35HT Inferno) |
Injection: | A) Split 50:1 @ 350 °C, 1 µLB) Split 50:1 @ 300 °C, 1 µL |
Carrier Gas: | Helium @ 2.1 mL/min (constant flow) |
Oven Program: | A) 140 °C to 400 °C @ 10 °C/minB) 140 °C to 300 °C @ 10 °C/min |
Sample: | 1. Hexadecylamine |
Note: | Chromatogram is courtesy of Northeastern Chemical Company. |
Well-Suited for Environmental Contaminants
PAHs and PCBs In A Single Run
Column: | Zebron ZB-35 Inferno |
Dimension: | 30 meter x 0.25 mm x 0.25 µm |
Detector: | MSD @ 280 °C |
Part No.: | 7HG-G025-11 |
Injection: | Splitless @ 265 °C, 2 µL |
Carrier Gas: | Helium @ 1 mL/min (constant flow) |
Oven Program: | 85 °C for 3 min to 320 °C @ 7 °C /minfor 8 min |
Sample:
Compounds are 5 ppm
1. Naphthalene
2. Acenaphthylene
3. Acenaphthene
4. Fluorene
5. Phenanthrene
6. Anthracene
7. PCB 28
8. PCB 52
9. PCB 101
10. Fluoranthene
11. Pyrene
12. PCB 118
13. PCB 153
14. PCB 138
15. PCB 180
16. Benz[a]anthracene
17. Chrysene
18. PCB 194
19. Benzo[b]fluoranthene
20. Benzo[k]fluoranthene
21. Benzo[a]pyrene
22. Indeno[1,2,3-cd]pyrene
23. Dibenz[a,h]anthracene
24. Benzo[g,h,I]perylene
Documents
- Guide: Zebron GC Column Selection Chart
- Brochures: Zebron Gas Management Brochure
- Supporting Docs: Zebron Gas Filter Selection Tool
- Supporting Docs: Zebron Gas Filter User Guide
- Technical Notes: GCxGC-VUV and GCxGC-FID Analysis of Gasoline, Middle Distillates and Crude Oil Distillation Cuts using Zebron ZB-35HT and ZB-1plus GC Columns (TN-2089)
- Technical Notes: Orthogonal Selectivity for Separation of Light and Heavy Petroleum Hydrocarbons by 2D GC using Zebron ZB-1HT Inferno and ZB-35HT Inferno GC Columns (TN-2085)
- Brochures: Chemical Industry LC & GC Separation Solutions Guide
FAQs
Can I pack or re-pack my GC liner with wool?
Though the upfront cost of self-packing your liner may seem attractive, the time and headaches caused by resulting tailing or irreproducible peaks can be sizeable! Self-packed wool fibers commonly break during installation and any existing deactivation on the liner can also be scratched or damaged. Scratches in the deactivation layer are likely to occur when removing wool from the liner or re-packing it with new wool. Also, when wool is forcefully inserted or removed, these scratches could expose active sites, resulting in peak tailing and poor reproducibility. Pre-packed Zebron PLUS liners undergo the deactivation process with the quartz wool already in place, which ensures that any active sites that form during packing are not exposed. Its novel touchless packaging and preinstalled O-ring prevent contamination during installation.
Does the Zebron PLUS liner with wool improve my GC column lifetime?
Yes. Zebron PLUS liners are packed with quartz wool, which serves two purposes: a) Quartz wool promotes homogenous vaporization of analytes and solvent in the inlet to effectively transfer them to the head of the GC column. b) Quartz wool acts as a filter, trapping non-volatile impurities and preventing them from proceeding further into the GC column.
I work with dirty samples which produce a residue on my GC liner after approximately 100 injections. Can I scrub/sonicate my liner and reuse it?
It is not recommended to scrub/sonicate your liners. Residue formation indicates contamination. More specifically, this shows that the sample contains non-volatile impurities, in which case it is recommended to replace your liner rather than clean it. Sonication can alter the liner’s deactivation, and scrubbing can create scratches and active sites. As a result, you can have several chromatography problems such as poor quantitation, analyte breakdown, poor reproducibility, peak asymmetry, etc.
Is there a way I can get immediate help with my current and upcoming method?
Absolutely, we're always here to help! You can easily get in contact with our team members by clicking contact us on the menu or better yet, just head to www.phenomenex.com/chatnow and we'll help you out with method recommendations and tips.
I am using an inert GC column for my analysis, and I still see peak tailing. What could be the reason for this?
For analysis of active compounds, it is crucial to use both a highly inert column and a highly inert liner. The liner is the first place of potential analyte interaction during GC analysis; it is important that your analytes are not adsorbed. Zebron PLUS liners undergo a rigorous deactivation process and are tested for inertness to ensure reliable results when working with highly active compounds such as underivatized acids and active bases.
When facing peak and resolution issues in sample analysis by GC, where is the best place to start?
The inlet is the most common place where problems happen in gas chromatography. This is because: • The inlet is subjected to very high temperatures. • There are multiple consumables involved in the inlet that need routine maintenance. • Some inlet modes, such as splitless injection, are a slow process, meaning that target analytes and the inlet can interact with each other before the sample enters the column.
Can you recommend a GC liner that work best when analyzing dirty samples, samples with wide boiling points, or samples with wide molecular weight?
Analysis of dirty samples, samples with wide boiling points, or samples with wide molecular weights can be enhanced by choosing a Zebron™ PLUS liner with quartz wool. Liners packed with wool can prevent non-volatile compounds from entering the column and improve sample vaporization for a more robust, reproducible analysis.
Manufacturer information: Zebron ZB-35HT Inferno GC Columns – Phenomenex (USA). MAS Brand is the official representative of Phenomenex in Egypt.
Specifications for Zebron ZB-35HT GC Columns
| GC Length (m) | 0.5 or 1 or 1.5 or 5 or 15 or 20 or 30 |
| GC Internal Diameter (mm) | 0.1 or 0.18 or 0.25 or 0.32 or 0.53 |
| GC Film Thickness (µm) | 0.05 or 0.07 or 0.1 or 0.15 or 0.18 or 0.25 |
| GC Format | Guard Column or Capillary Column or 5-inch Cage |
| GC Option | Standard or w/ GUARDIAN 5 m, Custom or Dual Integrated Guard |
| Manufacturer | Phenomenex |
| GC Phase | ZB-35HT |